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This is the final formal lab activity of the chemistry
Typology: Lab Reports
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THE FINAL FORMAL LAB ACTIVITY of the Chemistry 11 Course
A titration is an analytical procedure used to determine the accurate concentration of a sample by reacting it with a standard solution. One type of titration uses a neutralization reaction, in which an acid and a base react to produce a salt and water: In equation 1, the acid is HCl (hydrochloric acid) and the base is NaOH (sodium hydroxide). When the acid and base react, they form NaCl (sodium chloride), which is also known as table salt. The titration proceeds until the equivalence point is reached, where the number of moles of acid (H
) is equal to the number of moles of base (OH
A buret is used because the volumes can be measured very precisely ( + 0.05 mL). ( + ½ of the marking on the glassware). Be sure you are reading volumes properly, from the bottom of the meniscus. For example the volume on the buret below would be 18.50 + 0.05 mL If this was your final volume reading on your buret, it would be 42.30 + 0.05 mL This volume information would be written in a data table like this: INITIAL BURET READING: 18.50 + 0.05 mL. FINAL BURET READING: 42.30 + 0.05 mL TOTAL VOLUME OF NaOH used in the Titraion: Vf – Vi = 42.30 – 18.50 = 23.80 ml The acid is typically added to the Erlenmeyer flask in a specific volume (usually 10.0 or 25.0 mL) using a pipette which also measures volumes very precisely. The sample size (in mL) of the unknown is called an “aliquot.” A typical pipette
Use a beaker filled with H 2 O to perform these rinses and then dump the water rinsings into the sink)
You will likely NOT be successful the first time you try this, as you have no idea how many mL of NaOH it will take to neutralize your unknown acid sample. Consider the following tips:
Drain the NaOH out of the burette (discard unused solutions in waste container), and rinse the burette with water before putting it away. YOU CAN NOT LEAVE any NaOH inside the buret!!!! Neutralized solution in the Erlenmeyer flask can be rinsed down the drain with H 2 O Rinse all glassware with water and put all glassware away (does not have to be dried).
If you are starting this lab on the next day, repeat steps 1 to 4 from the DAY ONE instructions.