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To construct heating and cooling curves of a pure substance using experimental data. • To determine the freezing and melting point temperatures of the pure ...
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Purpose: To understand that a phase change is a physical change. To practice techniques of heating materials using the Bunsen burner. To study the effects of heating and cooling a pure substance through a change of phase. To construct heating and cooling curves of a pure substance using experimental data. To determine the freezing and melting point temperatures of the pure substance. Discussion: In this laboratory investigation you will take Stearic Acid and determine its freezing point and melting point experimentally. When the data collection is completed, your graph should reflect pictorially what happens to a pure substance as its temperature is raised and lowered over a temperature interval that includes its freezing and melting points. The graph will also show how the freezing and melting points of a pure substance are related. Safety: Goggles and Aprons Equipment: Sample test tube containing Stearic Acid Goggles Apron Beaker – 400 mL Thermometer Ring stand Iron ring Wire gauze Test tube clamp Test tube rack Bunsen burner Stop watch/timer with second hand Material: Steric Acid Test Tube Water
STEP ONE: Preparation for cooling curve: Before any data can be taken the Stearic Acid test tube must be prepared. It is given to you by the teacher in the solid phase. Therefore, it is below its freezing point. We must first melt the sample in a hot water bath to prepare it for the cooling curve data.
Plot your data from this experiment on the set of axes in the graph below. Use a blue pencil to plot cooling data and a red pencil to plot heating data.